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During the sulphated ash test, constant weight refers to achieving a stable mass of the sample after it has been ignited to remove any organic material and drive off volatile substances. This step ensures that all organic components have been effectively burned off, leaving behind only the inorganic residues for accurate measurement. Constant weight indicates that the sample has reached a point where no further change in mass occurs, confirming complete combustion.

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Q: What is constant weight during sulphated ash test?
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Related questions

Why used sulfuric acid in sulphated ash test?

Sulfuric acid is used in the sulphated ash test to convert the inorganic components present in the sample to their sulfates. This step helps in ensuring complete combustion of organic material and facilitates the determination of the ash content accurately. The use of sulfuric acid also helps in removing any carbon residues that may be present in the sample.


What is sulphated ash?

The sulphated ash test is an analytical test for determining the inorganic content of a sample by weight. The sample ( usually 1g) is accurately weighed into a platinum, silica crucible that has been previously ignited, cooled and weighed. The sample in the crucible is then subjected to sulphuric acid (usually 1mL) and charred at a low temperature without causing ignition of the sample until there are no more white fumes given off. The crucible with the charred sample is then placed in a furnace (temperature is dependent on monograph but typically it can be from 600 to 900 degrees celcius) until all organic matter has been burnt off. The crucible is cooled and re-weighed. The difference in sample weights being the sulphated ash content remaining. Some monographs require the sample to be re-ashed until a constand weight has been achieved. The remaining inorganic matter is typically metal oxides from most samples.


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